| 摘要: |
| 对气相色谱-质谱法(GC/MS)测定猪肝中盐酸克仑特罗残留的不确定度进行评定。通过对测定过程中各变量的分析，确定了不确定度来源，建立了数学模型，计算出了各变量的不确定度,最后计算出合成不确定度。当猪肝中盐酸克仑特罗残留量为5.10 μg/kg时，测定结果的扩展不确定度为0.15μg/kg（k=2）。 |
| 关键词: 不确定度 气相色谱-质谱 盐酸克仑特罗 残留 猪肝 |
| DOI： |
| 投稿时间：2008-06-13修订日期：2008-07-28 |
| 基金项目: |
|
| Uncertainty Evaluation in the Determination of Clenbuterol hydrochloride in Swine Liver by Gas Chromatography－Mass Spectrometry |
| zhuxinle |
| (China Institute of Veterinary Drug Control) |
| Abstract: |
| The uncertainty of determination of clenbuterol hydrochloride residue in swine liver by GC/MS was evaluated． By analyzing the various variable parameters among the procedures， the components of uncertainty were identified, the mathematical model was established, and every components of uncertainty was calculuated , thereby the combined uncertainty was finally obtained. The expanded uncertainty was 0.15μg/kg（k=2）with 5.10μg/kg of the content of clenbuterol hydrochloride residue in swine liver. |
| Key words: uncertainty Gas Chromatography-Mass Spectrometry clenbuterol hydrochloride residue swine liver |
