| 摘要: |
| 建立了苦参苍术口服液中三氯甲烷残留量的气相色谱检测方法，采用DB-FFAP毛细管柱，柱温为程序升温，氢火焰离子化检测器（FID），检测器温度为250 ℃，进样口温度为220 ℃，载气为氮气。试验结果三氯甲烷在6.0464～120.928 μg/mL浓度范围内呈良好的线性关系(r=0.99995)，加样回收实验平均回收率为98.01%（RSD=1.6%）。本方法简便、快速、准确、重现性好，可作为苦参苍术口服液中三氯甲烷残留量的检测方法。 |
| 关键词: 气相色谱法 苦参苍术口服液 三氯甲烷 |
| DOI： |
| 投稿时间：2013-10-31修订日期：2014-01-26 |
| 基金项目:“十一五”国家科技支撑计划“中兽药现代化技术研究与开发”（2008BADB4B04） |
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| Determination of Chloroform Residue in Kushencangzhu Oral Liquid by Gas Chromatography |
|
| (China Institute of veterinary Drug Control) |
| Abstract: |
| To establish a gas chromatography method for the determination of chloroform residue in Kushencangzhu oral liquid. Chloroform was determined on DB-FFAP capillary column using temperature programming. FID was used as detector with a temperature of 250 ℃, and the temperature of sample injection was 220 ℃, nitrogen was used as carrier gas. The linear range of chloroform was 6.0464～120.928 μg/mL（r＝0.99995）. The average recovery was 98.1％（RSD＝1.6％）. The method is simple, fast, accurate and reproducible, it can be used for the determination of residual chloroform in Kushenangzhu oral liquid. |
| Key words: gas chromatography Kushencangzhu oral liquid chloroform |
